3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid

Base Information

• Chemical Name: 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid
• CAS No.: 145126-18-7
• Molecular Formula: C₁₆H₂₁NO₆
• Molecular Weight: 323.346

Synonyms:3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid

Chemical Property of 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid

Chemical Property:

Purity/Quality:

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Technology Process of 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid

There total 1 articles about 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid (145126-18-7)

Guidance literature:

Boc-N3, Asp-OBz;

DOI:10.1021/bi00851a040

Reference yield: 100.0%

DL-α,β-distearin (51063-97-9) + 3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid (145126-18-7) → 1-benzyl 4-(2,3-bis(stearoyloxy)propyl) (tert-butoxycarbonyl)aspartate

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h;

Reference yield: 95.0%

3-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo-4-(phenylmethoxy)-butanoic acid (145126-18-7) + phenylhydrazine (100-63-0) → Boc-Asp-NH2-NH-Ph (145126-30-3)

Guidance literature:

In ethanol; at 35 ℃; for 5h; industrial alkaline protease alcalase;

DOI:10.1021/jo00051a052

Downstream raw materials:

Boc-Asp-NH₂-NH-Ph

L-aspartic acid beta-benzyl ester

C₁₇H₂₃NO₆

C₂₂H₃₂N₂O₅

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