1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

Base Information

Chemical Name:1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin
CAS No.:33566-97-1
Molecular Formula:C₂₀H₂₅NO₄
Molecular Weight:343.423
Hs Code.:

Synonyms:1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

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Chemical Property of 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

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Technology Process of 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

There total 5 articles about 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115032-11-6
1-(3,4-Dimethoxyphenyl)-4,5-dihydro-7,8-dimethoxy-3H-2-benzazepin

: 33566-97-1
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h; Heating;

Reference yield:

: 14773-42-3
3-(3,4-dimethoxyphenyl)propylamine

: 33566-97-1
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / C₅H₅N / CHCl₃ / 1 h / Ambient temperature

2: POCl₃ / acetonitrile / 20 h / Heating

3: NaBH₄ / methanol / 0.5 h / Heating

With pyridine; sodium tetrahydroborate; trichlorophosphate; In methanol; chloroform; acetonitrile;

Reference yield:

: 115032-00-3
N-<3-(3,4-Dimethoxyphenyl)propyl>-3,4-dimethoxybenzamid

: 33566-97-1
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃ / acetonitrile / 20 h / Heating

2: NaBH₄ / methanol / 0.5 h / Heating

With sodium tetrahydroborate; trichlorophosphate; In methanol; acetonitrile;