1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

Base Information

Chemical Name:1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat
CAS No.:115032-07-0
Molecular Formula:C₂₀H₂₅NO₄*ClHO₄
Molecular Weight:443.881
Hs Code.:

Synonyms:1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

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Chemical Property of 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

Chemical Property:

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Technology Process of 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

There total 5 articles about 1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 33566-97-1
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin

: 115032-07-0
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

Guidance literature:: With perchloric acid; In hydrogenchloride; water; Heating;

Reference yield:

: 14773-42-3
3-(3,4-dimethoxyphenyl)propylamine

: 115032-07-0
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / C₅H₅N / CHCl₃ / 1 h / Ambient temperature

2: POCl₃ / acetonitrile / 20 h / Heating

3: NaBH₄ / methanol / 0.5 h / Heating

4: 81 percent / 70 percent HClO₄ / H₂O; HCl / Heating

With pyridine; sodium tetrahydroborate; perchloric acid; trichlorophosphate; In hydrogenchloride; methanol; chloroform; water; acetonitrile;

Reference yield:

: 115032-00-3
N-<3-(3,4-Dimethoxyphenyl)propyl>-3,4-dimethoxybenzamid

: 115032-07-0
1-(3,4-Dimethoxyphenyl)-2,3,4,5-tetrahydro-7,8-dimethoxy-1H-2-benzazepin-hydroperchlorat

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃ / acetonitrile / 20 h / Heating

2: NaBH₄ / methanol / 0.5 h / Heating

3: 81 percent / 70 percent HClO₄ / H₂O; HCl / Heating

With sodium tetrahydroborate; perchloric acid; trichlorophosphate; In hydrogenchloride; methanol; water; acetonitrile;