C₂₀H₃₆O₂C₆H₆OCOC₆H₃ICH₂

Base Information

• Chemical Name: C₂₀H₃₆O₂C₆H₆OCOC₆H₃ICH₂
• CAS No.: 947243-86-9
• Molecular Formula: C₃₄H₄₇IO₄
• Molecular Weight: 646.649
• Mol file: 947243-86-9.mol

Synonyms:C₂₀H₃₆O₂C₆H₆OCOC₆H₃ICH₂

Chemical Property of C₂₀H₃₆O₂C₆H₆OCOC₆H₃ICH₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₀H₃₆O₂C₆H₆OCOC₆H₃ICH₂

There total 2 articles about C₂₀H₃₆O₂C₆H₆OCOC₆H₃ICH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl 18αH-scalar-16α-ol-17(20)-en-19-oate + 3-iodophenylacetic acid chloride (127109-66-4) → C20H36O2C6H6OCOC6H3ICH2 (947243-86-9)

Guidance literature:

With pyridine; In benzene; for 4h; Heating;

DOI:10.1016/j.tet.2007.05.048

Reference yield:

3-iodophenylacetic acid (1878-69-9) → C20H36O2C6H6OCOC6H3ICH2 (947243-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 0.5 h / Heating

2: 99 percent / pyridine / benzene / 4 h / Heating

With pyridine; thionyl chloride; In N,N-dimethyl-formamide; benzene;

DOI:10.1016/j.tet.2007.05.048

Reference yield:

C20H36O2C6H6OCOC6H3ICH2 (947243-86-9) → C20H36O2C6H6OCOC6H2IClCH2

Guidance literature:

With sulfuryl dichloride; dibenzoyl peroxide; In tetrachloromethane; for 5h; Heating;

DOI:10.1016/j.tet.2007.05.048

upstream raw materials:

3-iodophenylacetic acid chloride

3-iodophenylacetic acid