C₅₄H₅₄S₄

Base Information

• Chemical Name: C₅₄H₅₄S₄
• CAS No.: 1352833-76-1
• Molecular Formula: C₅₄H₅₄S₄
• Molecular Weight: 831.287
• Mol file: 1352833-76-1.mol

Synonyms:C₅₄H₅₄S₄

Chemical Property of C₅₄H₅₄S₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₅₄S₄

There total 4 articles about C₅₄H₅₄S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-tert-Butyl-m-xylene (98-19-1) → C54H54S4 (1352833-76-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / Methyl formate / 3 h

2.1: potassium carbonate / tetrahydrofuran / 20 h / Inert atmosphere; Reflux

3.1: potassium thioacetate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; potassium carbonate; potassium thioacetate; In tetrahydrofuran; Methyl formate; mineral oil;

DOI:10.1002/chem.201101837

Reference yield:

1,3,5-Tris(bromomethyl)benzene (18226-42-1) → C54H54S4 (1352833-76-1)

Guidance literature:

Multi-step reaction with 3 steps

1: lithium chloride / N,N-dimethyl-formamide / 2.5 h / 0 - 20 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; lithium chloride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;

DOI:10.1002/chem.201101837

Reference yield:

α,α',α''-trichloromesitylene (17299-97-7) → C54H54S4 (1352833-76-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; mineral oil;

DOI:10.1002/chem.201101837

upstream raw materials:

5-tert-Butyl-m-xylene

1,3,5-Tris(bromomethyl)benzene

α,α',α''-trichloromesitylene

5-tert-butyl-1,3-bis(bromomethyl)benzene

Downstream raw materials:

C₃₅H₄₀S₄

C₈₂H₉₄S₈

Refernces