perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane

Base Information

• Chemical Name: perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane
• CAS No.: 119022-47-8
• Molecular Formula: C₉F₁₄O₅
• Molecular Weight: 454.074
• Mol file: 119022-47-8.mol

Synonyms:perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane

Chemical Property of perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane

There total 1 articles about perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

Hexafluoropropene oxide (428-59-1,25038-02-2) + 4-fluoro-5-oxo-2,4-bis(trifluoromethyl)-1,3-dioxolane-2-carbonyl fluoride (7345-49-5) → perfluoro(2-propoxypropionyl) fluoride (2062-98-8,125037-08-3,75566-60-8) + perfluoro-2-oxo-3,6-dimethyl-1,4-dioxane (7309-84-4) + perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane (119022-47-8)

Guidance literature:

With cesium fluoride; In diethylene glycol dimethyl ether; for 2h;

DOI:10.1007/BF00957432

Reference yield:

perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane (119022-47-8) → perfluoro(2-propoxypropionyl) fluoride (2062-98-8,125037-08-3,75566-60-8) + perfluoro-2-oxo-3,6-dimethyl-1,4-dioxane (7309-84-4)

Guidance literature:

With Hexafluoropropene oxide; cesium fluoride; In diethylene glycol dimethyl ether; at 20 ℃; for 1h;

DOI:10.1007/BF00957432

Reference yield:

perfluoro-4-oxo-2,5-dimethyl-2-(2'-oxa-3'-fluorocarbonylbutyl)-1,3-dioxolane (119022-47-8) → perfluoro-2-oxo-3,6-dimethyl-1,4-dioxane (7309-84-4) + 4-fluoro-5-oxo-2,4-bis(trifluoromethyl)-1,3-dioxolane-2-carbonyl fluoride (7345-49-5)

Guidance literature:

With cesium fluoride; In diethylene glycol dimethyl ether; at 20 ℃; for 0.166667h; under 3750.3 Torr;

DOI:10.1007/BF00957433

upstream raw materials:

Hexafluoropropene oxide

4-fluoro-5-oxo-2,4-bis(trifluoromethyl)-1,3-dioxolane-2-carbonyl fluoride

Downstream raw materials:

perfluoro(2-propoxypropionyl) fluoride

perfluoro-2-oxo-3,6-dimethyl-1,4-dioxane

4-fluoro-5-oxo-2,4-bis(trifluoromethyl)-1,3-dioxolane-2-carbonyl fluoride