veratric acid p-anisidide

Base Information

• Chemical Name: veratric acid p-anisidide
• CAS No.: 1718-92-9
• Molecular Formula: C₁₆H₁₇NO₄
• Molecular Weight: 287.315
• Mol file: 1718-92-9.mol

Synonyms:veratric acid p-anisidide

Chemical Property of veratric acid p-anisidide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of veratric acid p-anisidide

There total 2 articles about veratric acid p-anisidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-aniline (104-94-9) + 3,4-dimethoxybenzoic acid chloride (3535-37-3) → veratric acid p-anisidide (1718-92-9)

Guidance literature:

With benzene;

DOI:10.1021/ja01180a033

Reference yield:

(3,4-dimethoxybenzylidene)-(4-methoxyphenyl)amine (82363-24-4) → veratric acid p-anisidide (1718-92-9)

Guidance literature:

With sulfuryl dichloride; water; Yield given. Multistep reaction; 1.) acetonitrile, 0 deg C, 10 min, 2.) r.t., 20 min;

Reference yield: 87.0%

veratric acid p-anisidide (1718-92-9) → 3,4-dimethoxy-N-(4-methoxyphenyl)benzothioamide (156085-97-1)

Guidance literature:

With Lawessons reagent; In chlorobenzene; for 3h; Heating;

DOI:10.1021/jm00037a020

upstream raw materials:

4-methoxy-aniline

3,4-dimethoxybenzoic acid chloride

(3,4-dimethoxybenzylidene)-(4-methoxyphenyl)amine

Downstream raw materials:

3,4-dimethoxy-N-(4-methoxyphenyl)benzothioamide

Refernces

• 1、 Dhar, Durga N.,Gupta, Sudha R.. "Reaction of Sulphuryl Chloride with Some Schiff Bases". . p. 533 - 535. Retrieved 2007/10/02.