N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

Base Information

Chemical Name:N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide
CAS No.:1423077-22-8
Molecular Formula:C₂₂H₁₈ClN₃O₂S₂
Molecular Weight:455.989
Hs Code.:

Synonyms:N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

Chemical Property:

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Technology Process of N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

There total 3 articles about N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 3763-80-2
3-(2-chloro-10H-phenothiazin-10-yl)propan-1-amine hydrochloride

: 49584-26-1
p-cyanobenzenesulfonyl chloride

: 1423077-22-8
N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 2h;

Reference yield:

: 180388-71-0
N-[3-(2-chloro-phenothiazin-10-yl)-propyl]-phthalimide

: 1423077-22-8
N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; hydrazine / ethanol; 1,4-dioxane

2: triethylamine / N,N-dimethyl-formamide / 2 h / 0 - 25 °C

With hydrogenchloride; triethylamine; hydrazine; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2015.07.007

Reference yield:

: 92-39-7
2-chlorophenothiazine

: 1423077-22-8
N-(3-(2-chloro-10H-phenothiazin-10-yl)propyl)-4-cyanobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil

2: hydrogenchloride; hydrazine / ethanol; 1,4-dioxane

3: triethylamine / N,N-dimethyl-formamide / 2 h / 0 - 25 °C

With hydrogenchloride; sodium hydride; triethylamine; hydrazine; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmc.2015.07.007