N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

Base Information

Chemical Name:N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide
CAS No.:192461-82-8
Molecular Formula:C₂₃H₂₂NO₂P
Molecular Weight:375.407
Hs Code.:

Synonyms:N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

Chemical Property:

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Technology Process of N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

There total 1 articles about N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54951-36-9
6-methoxy-1-tetralone oxime

: 1499-21-4
Diphenylphosphinic chloride

: 192461-82-8
N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

Guidance literature:: DOI:10.1002/chem.200304794

Reference yield: 97.0%

: 192461-82-8
N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

: 259729-26-5
(S)-N-(diphenylphosphinyl)-6-methoxy-1,2,3,4-tetrahydro-1-naphthylamine

Guidance literature:: With sodium tetrahydroborate; (S,S)-Co(II) complex catalyst (C₄₆H₅₀N₂O₄Co); In ethanol; chloroform; at 0 ℃; for 4h;
DOI:10.1246/cl.1997.493

Reference yield:

: 192461-82-8
N-(6-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)-P,P-diphenylphosphinamide

: 314019-11-9
(S)-6-methoxy-1,2,3,4-tetrahydro-1-naphthylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaBH₄+tetrahydrofurfuryl alcohol / (S,S)-Co(II) complex catalyst (C₄₆H₅₀N₂O₄Co) / ethanol; CHCl₃ / 4 h / 0 °C

2: HCl / methanol / 3 h / 25 °C

With hydrogenchloride; sodium tetrahydroborate; (S,S)-Co(II) complex catalyst (C₄₆H₅₀N₂O₄Co); In methanol; ethanol; chloroform;
DOI:10.1246/cl.1997.493