cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

Base Information

Chemical Name:cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol
CAS No.:79076-07-6
Molecular Formula:C₂₇H₂₇NO₃
Molecular Weight:413.516
Hs Code.:

Synonyms:cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

Chemical Property:

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Technology Process of cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

There total 8 articles about cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 79076-08-7,79076-09-8
(1S,2S)-2-(Benzhydrylidene-amino)-1-(1-benzo[1,3]dioxol-5-yl-vinyl)-cyclopentanol

: 79076-07-6
cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

Guidance literature:: With sodium cyanoborohydride; In ethanol;
DOI:10.1021/ja00408a055

Reference yield:

: 119-61-9
benzophenone

: 79076-07-6
cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / monohydrated p-toluenesulfonic acid / toluene / 18 h / Heating

2: 1.) Me₂SO, oxalyl chloride, 2.) Et₃N / 1.) methylene dichloride, -60 deg C to -50 deg C, 25 min, 2.) -60 deg C to -50 deg C, 5 min, then to room temperature

3: 1.) t-BuLi, 3.) NaCNBH₃, 1N HCl / 1.) pentane, ether, -78 deg C, 1 h, 2.) ether, -78 deg C, 2 h, 3.) methanol, reflux, 21 h

With hydrogenchloride; oxalyl dichloride; tert.-butyl lithium; sodium cyanoborohydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In toluene;
DOI:10.1021/ja00360a014

Reference yield:

: 33092-86-3
trans-2-aminocyclopentanol

: 79076-07-6
cis-2-((diphenylmethyl)amino)-1-<1-(3,4-(methylendioxy)phenyl)ethenyl>cyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / monohydrated p-toluenesulfonic acid / toluene / 18 h / Heating

2: 1.) Me₂SO, oxalyl chloride, 2.) Et₃N / 1.) methylene dichloride, -60 deg C to -50 deg C, 25 min, 2.) -60 deg C to -50 deg C, 5 min, then to room temperature

3: 1.) t-BuLi, 3.) NaCNBH₃, 1N HCl / 1.) pentane, ether, -78 deg C, 1 h, 2.) ether, -78 deg C, 2 h, 3.) methanol, reflux, 21 h

With hydrogenchloride; oxalyl dichloride; tert.-butyl lithium; sodium cyanoborohydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In toluene;
DOI:10.1021/ja00360a014