(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

Base Information

Chemical Name:(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide
CAS No.:126333-90-2
Molecular Formula:BrH*C₁₃H₁₉Cl₂N₃O
Molecular Weight:385.131
Hs Code.:

Synonyms:(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

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Technology Process of (S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

There total 2 articles about (S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 126453-28-9
{(S)-1-[N',N'-Bis-(2-chloro-ethyl)-hydrazinocarbonyl]-2-phenyl-ethyl}-carbamic acid benzyl ester

: 126333-90-2
(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 1h; Ambient temperature;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 126333-90-2
(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 69.1 percent / DCC / CHCl₃ / Ambient temperature; 1) 0 degC, 4 h; 2) 1 h, room temp.

2: 93 percent / 33 percent HBr / acetic acid / 1 h / Ambient temperature

With hydrogen bromide; dicyclohexyl-carbodiimide; In chloroform; acetic acid;