(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

Base Information

Chemical Name:(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride
CAS No.:126333-91-3
Molecular Formula:C₁₃H₁₉Cl₂N₃O*ClH
Molecular Weight:340.68
Hs Code.:

Synonyms:(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

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Chemical Property of (S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

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Technology Process of (S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

There total 3 articles about (S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 126333-90-2
(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrobromide

: 126333-91-3
(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 1h;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 126333-91-3
(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 69.1 percent / DCC / CHCl₃ / Ambient temperature; 1) 0 degC, 4 h; 2) 1 h, room temp.

2: 93 percent / 33 percent HBr / acetic acid / 1 h / Ambient temperature

3: 89 percent / HCl / ethanol / 1 h

With hydrogenchloride; hydrogen bromide; dicyclohexyl-carbodiimide; In ethanol; chloroform; acetic acid;

Reference yield:

: 126453-28-9
{(S)-1-[N',N'-Bis-(2-chloro-ethyl)-hydrazinocarbonyl]-2-phenyl-ethyl}-carbamic acid benzyl ester

: 126333-91-3
(S)-2-Amino-3-phenyl-propionic acid N',N'-bis-(2-chloro-ethyl)-hydrazide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 33 percent HBr / acetic acid / 1 h / Ambient temperature

2: 89 percent / HCl / ethanol / 1 h

With hydrogenchloride; hydrogen bromide; In ethanol; acetic acid;