C₂₆H₂₉N₃O₅

Base Information

Chemical Name:C₂₆H₂₉N₃O₅
CAS No.:1355951-96-0
Molecular Formula:C₂₆H₂₉N₃O₅
Molecular Weight:463.533
Hs Code.:

C<sub>26</sub>H<sub>29</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₆H₂₉N₃O₅

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Chemical Property of C₂₆H₂₉N₃O₅

Chemical Property:

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Technology Process of C₂₆H₂₉N₃O₅

There total 15 articles about C₂₆H₂₉N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3740-52-1
2-(2-nitrophenyl)acetic acid

: 1355951-98-2
C₁₈H₂₄N₂O₂

: 1355951-96-0
C₂₆H₂₉N₃O₅

Guidance literature:: With bis(2-oxo-1,3-oxazolidin-3-yl)phosphinous chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1002/anie.201106205

Reference yield:

: 202753-56-8
2-(1H-4-bromoindol-3-yl)-ethanol

: 1355951-96-0
C₂₆H₂₉N₃O₅

Guidance literature:: Multi-step reaction with 14 steps

1.1: dmap; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0.17 h / 20 °C

2.2: 0.67 h / 20 °C

3.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

5.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

6.1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

7.1: toluene-4-sulfonic acid / 3 h / 20 °C

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

9.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 20 °C

11.1: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C

12.1: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

13.1: magnesium / methanol / 1 h / Sonication

14.1: bis(2-oxo-1,3-oxazolidin-3-yl)phosphinous chloride; triethylamine / dichloromethane / 12 h / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; thionyl chloride; sodium azide; bis(2-oxo-1,3-oxazolidin-3-yl)phosphinous chloride; tributylphosphine; methanesulfonamide; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; magnesium; mercaptoacetic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Heck reaction / 4.1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205

Reference yield:

: 1355951-84-6
C₂₈H₃₉NO₇S₂Si

: 1355951-96-0
C₂₆H₂₉N₃O₅

Guidance literature:: Multi-step reaction with 9 steps

1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

2: toluene-4-sulfonic acid / 3 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 12 h / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 20 °C

6: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C

7: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

8: magnesium / methanol / 1 h / Sonication

9: bis(2-oxo-1,3-oxazolidin-3-yl)phosphinous chloride; triethylamine / dichloromethane / 12 h / 0 - 20 °C

With dmap; lithium aluminium tetrahydride; sodium azide; bis(2-oxo-1,3-oxazolidin-3-yl)phosphinous chloride; tributylphosphine; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; toluene-4-sulfonic acid; magnesium; mercaptoacetic acid; triethylamine; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201106205