dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate

Base Information

Chemical Name:dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate
CAS No.:34265-97-9
Molecular Formula:C₁₆H₆F₈O₄
Molecular Weight:414.208
Hs Code.:

Synonyms:dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate

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Chemical Property of dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate

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Technology Process of dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate

There total 1 articles about dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 36629-42-2
methyl pentafluorobenzoate

: 34265-97-9
dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate

Guidance literature:: methyl pentafluorobenzoate; With tin(ll) chloride; zinc; In N,N-dimethyl-formamide; at 60 ℃; for 12h; Sealed tube;

With copper dichloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/acs.inorgchem.0c00576

Reference yield: 78.0%

: 34265-97-9
dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate

: 5216-23-9
2,2',3,3',5,5',6,6'-octafluoro-[1,1'-biphenyl]-4,4'-dicarboxylic acid

Guidance literature:: dimethyl 2,2',3,3',5,5',6,6'‐octafluoro‐[1,1'‐biphenyl]‐4,4'‐dicarboxylate; With potassium hydroxide; In tetrahydrofuran; methanol; at 25 ℃; for 1h;

With trifluoroacetic acid; In tetrahydrofuran; methanol; at 25 ℃; for 0.5h;
DOI:10.1021/jacs.8b05765