dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

Base Information

Chemical Name:dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate
CAS No.:226919-69-3
Molecular Formula:C₄₁H₆₁O₉PSi
Molecular Weight:756.989
Hs Code.:

Synonyms:dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

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Chemical Property of dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

Chemical Property:

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Technology Process of dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

There total 6 articles about dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 994-30-9
triethylsilyl chloride

: Phosphoric acid (3R,4R,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-hydroxy-tetrahydro-pyran-2-yl ester dibutyl ester

: 226919-69-3
dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

: dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-α-D-glucopyranoside phosphate

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ja016227r

Reference yield:

: 1011723-04-8
glucal epoxide

: 226919-69-3
dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / -78 °C

2: imidazole / tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol9905452

Reference yield:

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 226919-69-3
dibutyl 3,4,6-tri-O-benzyl-2-O-triethylsilyl-β-D-glucopyranoside phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyldioxirane / CH₂Cl₂; acetone / 0.25 h / 0 °C

2: CH₂Cl₂ / 0.33 h / -78 °C

3: imidazole / tetrahydrofuran / 2 h / 20 °C

With 1H-imidazole; 3,3-dimethyldioxirane; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ja016227r