1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

Base Information

Chemical Name:1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid
CAS No.:1356054-86-8
Molecular Formula:C₁₂H₈BClFN₃O₂
Molecular Weight:291.477
Hs Code.:

Synonyms:1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

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Chemical Property of 1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

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Technology Process of 1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

There total 2 articles about 1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356054-85-7
1-(3-chloro-5-fluorophenyl)-4-iodo-1H-pyrazolo[3,4-b]pyridine

: 1356054-86-8
1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

Guidance literature:: With potassium acetate; bis(pinacol)diborane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dimethyl sulfoxide; at 85 - 105 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 1260890-58-1
(3-chloro-5-fluorophenyl)hydrazine

: 153034-82-3
[(fluoro-2-iodo-4)pyrid-3-yl]-carboxaldehyde

: 1356054-86-8
1-(3-chloro-5-fluorophenyl)-1H-pyrazolo[3,4-b]pyridin-4-ylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-pyrrolidin-2-one / 1.75 h / 185 °C / Inert atmosphere; capped

2: bis(pinacol)diborane; potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / dimethyl sulfoxide / 2.5 h / 85 - 105 °C / Inert atmosphere

With potassium acetate; bis(pinacol)diborane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1-methyl-pyrrolidin-2-one; dimethyl sulfoxide;