3-(4-methoxyphenyl)propionic acid ethanethiol ester

Base Information

Chemical Name:3-(4-methoxyphenyl)propionic acid ethanethiol ester
CAS No.:208453-06-9
Molecular Formula:C₁₂H₁₆O₂S
Molecular Weight:224.324
Hs Code.:

Synonyms:3-(4-methoxyphenyl)propionic acid ethanethiol ester

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Chemical Property of 3-(4-methoxyphenyl)propionic acid ethanethiol ester

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Technology Process of 3-(4-methoxyphenyl)propionic acid ethanethiol ester

There total 2 articles about 3-(4-methoxyphenyl)propionic acid ethanethiol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1929-29-9
3-(4-methoxyphenyl)propanoic acid

: 208453-06-9
3-(4-methoxyphenyl)propionic acid ethanethiol ester

Guidance literature:: With mixed anhydride;
DOI:10.1246/cl.2011.959

Reference yield: 50.44%

: 1929-29-9
3-(4-methoxyphenyl)propanoic acid

: 75-08-1
ethanethiol

: 208453-06-9
3-(4-methoxyphenyl)propionic acid ethanethiol ester

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 16h;
DOI:10.1002/chem.201801887

Reference yield: 95.0%

: 86318-61-8
(tert-butyldimethylsilyl)acetylene

: 208453-06-9
3-(4-methoxyphenyl)propionic acid ethanethiol ester

: 1-(tert-butyl-dimethyl-silanyl)-5-(4-methoxy-phenyl)-pent-1-yn-3-one

Guidance literature:: With copper(l) iodide; trifuran-2-yl-phosphane; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In N,N-dimethyl-formamide; at 50 ℃; for 1h;
DOI:10.1055/s-2003-40861