(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

Base Information

Chemical Name:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate
CAS No.:1248569-13-2
Molecular Formula:C₁₈H₂₈N₂O₂
Molecular Weight:304.433
Hs Code.:

Synonyms:(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

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Technology Process of (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

There total 1 articles about (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1248569-13-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

Guidance literature:

Reference yield: 84.0%

: 60754-50-9
8-iodooct-1-yne

: 1248569-13-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

: 1279724-00-3
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl oct-7-ynyl(2-(pyridin-2-yl)ethyl)carbamate

Guidance literature:: (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 1h; Inert atmosphere;

8-iodooct-1-yne; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 1248569-13-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

: 1279724-20-7
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 6-(1-(6-(2-amino-1H-imidazol-4-yl)hexyl)-1H-1,2,3-triazol-4-yl)hexyl(2-(pyridin-2-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: copper(II) sulfate; sodium L-ascorbate / ethanol; dichloromethane; water / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 16 h

With sodium hydride; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmcl.2010.12.057