tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

Base Information

Chemical Name:tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate
CAS No.:1279724-19-4
Molecular Formula:C₄₀H₆₄N₈O₄
Molecular Weight:720.999
Hs Code.:

tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

Synonyms:tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

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Chemical Property of tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

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Technology Process of tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

There total 7 articles about tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1279724-02-5
tert-butyl 2-amino-4-(6-azidohexyl)-1H-imidazole-1-carboxylate

: 1279724-00-3
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl oct-7-ynyl(2-(pyridin-2-yl)ethyl)carbamate

: 1279724-19-4
tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In ethanol; dichloromethane; water; at 20 ℃;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 1248569-13-2
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl-2-(pyridin-2-yl)ethylcarbamate

: 1279724-19-4
tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: copper(II) sulfate; sodium L-ascorbate / ethanol; dichloromethane; water / 20 °C

With sodium hydride; copper(II) sulfate; sodium L-ascorbate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmcl.2010.12.057

Reference yield:

: 135920-29-5
7-azidoheptanoyl chloride

: 1279724-19-4
tert-butyl 2-amino-4-(6-(4-(6-((((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)carbonyl)(2-(pyridin-2-yl)ethyl)amino)hexyl)-1H-1,2,3-triazol-1-yl)hexyl)-1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1 h / 0 °C

2: N,N-dimethyl-formamide / 48 h

3: copper(II) sulfate; sodium L-ascorbate / ethanol; dichloromethane; water / 20 °C

With copper(II) sulfate; sodium L-ascorbate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.057