P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene

Base Information

• Chemical Name: P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene
• CAS No.: 347192-80-7
• Molecular Formula: C₂₂H₂₂NO₂P
• Molecular Weight: 363.396
• Mol file: 347192-80-7.mol

Synonyms:P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene

Chemical Property of P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene

There total 3 articles about P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenylphosphine (603-35-0) → P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene (347192-80-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium / tetrahydrofuran / 2 h / 25 °C

1.2: ammonium chloride / tetrahydrofuran / 2 h

2.1: tetrahydrofuran

With lithium; In tetrahydrofuran; 2.1: Staudinger reaction;

DOI:10.1016/S0040-4020(01)00165-X

Reference yield:

P,P-diphenyl-P-(methyl)(N-methoxycabonyl)phosphazene (127802-81-7) + benzyl bromide (100-39-0) → P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene (347192-80-7)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -20 deg C, 2.) THF, -70 deg C;

DOI:10.1016/0040-4039(96)00401-7

Reference yield:

(2-phenylethyl)diphenylphosphane (5952-49-8) + azidoformiate de methyle (1516-56-9) → P,P-diphenyl-P-(2-phenylethyl)(N-methoxycabonyl)phosphazene (347192-80-7)

Guidance literature:

In tetrahydrofuran;

DOI:10.1016/S0040-4020(01)00165-X

upstream raw materials:

P,P-diphenyl-P-(methyl)(N-methoxycabonyl)phosphazene

benzyl bromide

(2-phenylethyl)diphenylphosphane

azidoformiate de methyle

Downstream raw materials:

P,P-diphenyl-P-(1-benzylpentyl)(N-methoxycabonyl)phosphazene