1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Base Information

• Chemical Name: 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane
• CAS No.: 76237-14-4
• Molecular Formula: C₇H₁₃N₇O₁₁
• Molecular Weight: 371.221

Synonyms:1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Chemical Property of 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

Chemical Property:

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Technology Process of 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane

There total 6 articles about 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

hexamethylenetetramine (100-97-0) + ethanolamine (141-43-5) → 1-acetoxy-2-nitro-2-aza-4-nitroxybutane (71545-63-6) + Hexahydro-1,3,5-trinitro-1,3,5-triazine (121-82-4,82030-42-0) + 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane (76237-14-4)

Guidance literature:

With nitric acid; In acetic anhydride; acetic acid; at 50 - 60 ℃; for 1.5h;

Reference yield: 75.0%

hexamethylenetetramine (100-97-0) + acetic anhydride (108-24-7) + ethanolamine (141-43-5) → 1-acetoxy-2-nitro-2-aza-4-nitroxybutane (71545-63-6) + Hexahydro-1,3,5-trinitro-1,3,5-triazine (121-82-4,82030-42-0) + 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane (76237-14-4)

Guidance literature:

With nitric acid; In acetic acid; at 50 - 60 ℃; for 1.5h;

Reference yield: 62.0%

1,3,5-tris(2-hydroxyethyl)-1,3,5-triazacyclohexane (4719-04-4) → 1-acetoxy-2-nitro-2-aza-4-nitroxybutane (71545-63-6) + Hexahydro-1,3,5-trinitro-1,3,5-triazine (121-82-4,82030-42-0) + 1-acetoxy-2,4,6-trinitro-2,4,6-triaza-8-nitroxyoctane (76237-14-4)

Guidance literature:

With ammonium nitrate; nitric acid; In chloroform; acetic anhydride; at 55 - 60 ℃; for 1h;

upstream raw materials:

N,N'-methylene-bis(oxazolidine)

1,3,5-tris(2-hydroxyethyl)-1,3,5-triazacyclohexane

acetic anhydride

hexamethylenetetramine

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