1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Base Information

Chemical Name:1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)
CAS No.:113524-02-0
Molecular Formula:C₃₆H₄₂ClN₂O₆P
Molecular Weight:665.166
Hs Code.:

Synonyms:1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

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Chemical Property of 1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Chemical Property:

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Technology Process of 1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

There total 13 articles about 1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 108-24-7
acetic anhydride

: 113524-00-8
1-hydroxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

: 113524-02-0
1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: In pyridine; for 16h;

Reference yield:

: 56021-31-9
4-chloro-3,5-dihydroxytoluene

: 113524-02-0
1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: Multi-step reaction with 12 steps

1: 86 percent / K₂CO₃ / butan-2-one / 5 h / Heating

2: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / 0 °C

3: 85 percent / K₂CO₃ / butan-2-one / 5 h / Heating

4: 97 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating; Irradiation

5: 98 percent / aq. AgNO₃ / 2-methoxy-ethanol / 0.5 h / Heating

6: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C

7: 84 percent / AlCl₃ / chlorobenzene / 0.75 h / Heating

8: 79 percent / HCl / 4 h / Heating

9: 86 percent / K₂CO₃ / butan-2-one / 16 h / Heating

10: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

11: 91 percent / NaBH₄ / methanol / 1 h / 0 °C

12: 97 percent / pyridine / 16 h

With hydrogenchloride; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; tetra-n-butylammonium permanganate; hexane; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;

Reference yield:

: 27971-69-3
2‐chloro‐1,3‐dimethoxy‐5‐methyl benzene

: 113524-02-0
1-acetoxy-1-(2,3,5-tribenzyloxy-4-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: Multi-step reaction with 11 steps

1: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / 0 °C

2: 85 percent / K₂CO₃ / butan-2-one / 5 h / Heating

3: 97 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating; Irradiation

4: 98 percent / aq. AgNO₃ / 2-methoxy-ethanol / 0.5 h / Heating

5: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C

6: 84 percent / AlCl₃ / chlorobenzene / 0.75 h / Heating

7: 79 percent / HCl / 4 h / Heating

8: 86 percent / K₂CO₃ / butan-2-one / 16 h / Heating

9: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

10: 91 percent / NaBH₄ / methanol / 1 h / 0 °C

11: 97 percent / pyridine / 16 h

With hydrogenchloride; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; tetra-n-butylammonium permanganate; hexane; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;