N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester
CAS No.:156662-02-1
Molecular Formula:C₂₁H₂₅Cl₂N₂O₁₀PS
Molecular Weight:599.383
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

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Chemical Property of N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

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Technology Process of N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

There total 7 articles about N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 64-17-5
ethanol

: 156662-01-0
N-(benzyloxycarbonyl)-O-<5,7-dichloro-2,3-dihydro-3-(methylsulfonyl)-2-oxo-1,3,2λ⁵-benzoxazaphosphol-2-yl>serin methyl ester

: 156662-02-1
N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

Guidance literature:: With 1-methyl-1H-imidazole; In dichloromethane; for 0.166667h;

Reference yield:

: 609-89-2
2,4-dichloro-6-nitrophenol

: 156662-02-1
N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / H₂ / PtO₂ / ethanol / 96 h / 20 °C / 750.06 Torr

2: Et₃N / CH₂Cl₂ / 12 h / 20 °C

3: 69 percent / 10percent NaOH / H₂O / 12 h / 65 °C

4: Et₃N / diethyl ether; benzene / 20 h / 20 °C

5: PCl₅ / benzene; CH₂Cl₂ / 12 h / 20 °C

6: 90 percent / Et₃N / benzene / 0.33 h / 0 °C

7: 98 percent / 1-methylimidazole / CH₂Cl₂ / 0.17 h

With 1-methyl-1H-imidazole; sodium hydroxide; phosphorus pentachloride; hydrogen; triethylamine; platinum(IV) oxide; In diethyl ether; ethanol; dichloromethane; water; benzene;

Reference yield:

: 527-62-8
2,4-dichloro-6-aminophenol

: 156662-02-1
N-(benzyloxycarbonyl)-O-<<2,4-dichloro-6-<(methylsulfonyl)amino>phenoxy>ethoxyphosphoryl>serin methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: 69 percent / 10percent NaOH / H₂O / 12 h / 65 °C

3: Et₃N / diethyl ether; benzene / 20 h / 20 °C

4: PCl₅ / benzene; CH₂Cl₂ / 12 h / 20 °C

5: 90 percent / Et₃N / benzene / 0.33 h / 0 °C

6: 98 percent / 1-methylimidazole / CH₂Cl₂ / 0.17 h

With 1-methyl-1H-imidazole; sodium hydroxide; phosphorus pentachloride; triethylamine; In diethyl ether; dichloromethane; water; benzene;