3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

Base Information

Chemical Name:3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine
CAS No.:1421822-99-2
Molecular Formula:C₂₄H₄₆N₆O₄SSi₂
Molecular Weight:570.904
Hs Code.:

Synonyms:3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

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Chemical Property of 3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

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Technology Process of 3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

There total 4 articles about 3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 919-30-2,29159-37-3
3-aminopropyltriethoxysilane

: 1421822-98-1
3-(2-chloroethylthio)-5-(4-chlorophenyl)-4H-1,2,4-triazole-4-amine

: 1421822-99-2
3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

Guidance literature:: 3-aminopropyltriethoxysilane; With iodine; magnesium; In tetrahydrofuran; for 0.5h;

3-(2-chloroethylthio)-5-(4-chlorophenyl)-4H-1,2,4-triazole-4-amine; In tetrahydrofuran; for 10.5h; Reflux;
DOI:10.1039/c2ra21135a

Reference yield:

: 38539-88-7
potassium p-chlorobenzoylhydrazinodithioformate

: 1421822-99-2
3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate monohydrate / methanol / 6 h / Reflux

2.1: potassium carbonate / acetonitrile

3.1: magnesium; iodine / tetrahydrofuran / 0.5 h

3.2: 10.5 h / Reflux

With hydrazine hydrate monohydrate; iodine; potassium carbonate; magnesium; In tetrahydrofuran; methanol; acetonitrile; 3.1: |Barbier Coupling Reaction;
DOI:10.1039/c2ra21135a

Reference yield:

: 536-40-3
4-chlorobenzoic acid hydrazide

: 1421822-99-2
3-(2-((3-aminopropyl)diethoxysilyl)ethylthio)-5-(4-((3-aminopropyl)diethoxy silyl)phenyl)-4H-1,2,4-triazol-4-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / Cooling

2.1: hydrazine hydrate monohydrate / methanol / 6 h / Reflux

3.1: potassium carbonate / acetonitrile

4.1: magnesium; iodine / tetrahydrofuran / 0.5 h

4.2: 10.5 h / Reflux

With hydrazine hydrate monohydrate; iodine; potassium carbonate; magnesium; potassium hydroxide; In tetrahydrofuran; methanol; acetonitrile; 4.1: |Barbier Coupling Reaction;
DOI:10.1039/c2ra21135a