2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Base Information

Chemical Name:2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine
CAS No.:850309-51-2
Molecular Formula:C₂₃H₂₀N₂O₃
Molecular Weight:372.423
Hs Code.:

Synonyms:2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

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Chemical Property of 2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

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Technology Process of 2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

There total 7 articles about 2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 2973-19-5
2-hydroxy-5-nitrobenzyl chloride

: 2-phenyl-3,3'-dimethyl-3H-indole

: 850309-51-2
2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Guidance literature:: In dichloromethane; acetonitrile;

Reference yield:

: 611-70-1
phenyl isopropyl ketone

: 850309-51-2
2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / AcOH / 17 h / Heating

2.1: acetonitrile / 0.83 h / 20 °C

2.2: 58 percent / KOH / H₂O

With acetic acid; In acetonitrile;
DOI:10.1021/jo051417w

Reference yield:

: 100-63-0
phenylhydrazine

: 850309-51-2
2-nitro-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / AcOH / 17 h / Heating

2.1: acetonitrile / 0.83 h / 20 °C

2.2: 58 percent / KOH / H₂O

With acetic acid; In acetonitrile;
DOI:10.1021/jo051417w