(4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde

Base Information

• Chemical Name: (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde
• CAS No.: 130796-31-5
• Molecular Formula: C₁₃H₁₆O₄
• Molecular Weight: 236.268

Synonyms:(4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde

Chemical Property of (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde

Chemical Property:

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Technology Process of (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde

There total 24 articles about (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(4R,5R)-cis-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde (130718-76-2) → (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde (130796-31-5)

Guidance literature:

With triethylamine; In dichloromethane; for 48h; Ambient temperature;

Reference yield: 94.0%

cis-4--2,2-dimethyl-5-(4-methoxyphenyl)-1,3-dioxolan (130718-85-3) → cis-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde (130718-76-2,130796-30-4,130796-31-5)

Guidance literature:

With boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; water; for 1h; Ambient temperature;

Reference yield: 67.0%

(4S,5R)-trans-4--5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan (130796-28-0) → (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde (130796-31-5)

Guidance literature:

With boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; water; for 1h; Ambient temperature;

upstream raw materials:

(4R,5R)-cis-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carbaldehyde

(4S,5R)-trans-4--5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan

methyl (R)-2-hydroxy-2-(4-methoxyphenyl)acetate

methyl (R)-2-(4-methoxyphenyl)-2-(trimethylsilyloxy)acetate

Downstream raw materials:

(4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carboxylic acid

(2S,3R)-(-)-methyl 2,3-dihydroxy-3-(p-methoxyphenyl)propionate

methyl (4S,5R)-trans-5-(4-methoxyphenyl)-2,2-dimethyl-1,3-dioxolan-4-carboxylate

methyl 2,3-dihydroxy-3-(4-methoxyphenyl)propanoate

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