{(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride

Base Information

Chemical Name:{(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride
CAS No.:86847-08-7
Molecular Formula:C₃₇H₃₀ClCuP₂
Molecular Weight:635.592
Hs Code.:

Synonyms:{(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride

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Chemical Property of {(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride

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Technology Process of {(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride

There total 1 articles about {(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 103559-83-7
hexaphenylcarbodiphosphorane

: copper(l) chloride

: 86847-08-7
{(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride

Guidance literature:: In tetrahydrofuran; at 20°C; filtration, crystn. at 0°C;

Reference yield: 65.0%

: 86847-08-7
{(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I) chloride

: 94348-92-2
potassium pentamethylcyclopentadiene

: 110354-18-2
(η5-pentamethylcyclopentadienyl){(triphenylphosphonio)(triphenylphosphoranylidene)methyl}copper(I)

Guidance literature:: In tetrahydrofuran; KC5Me5 was added portionwise to a THF soln. of Cu-complex under Ar, mixt. was stirred at 0°C for 2 h; carefully filtered through a layer of Na2SO3 (water cooling), concd., covered with a layer of pentane and stored at -15°C; elem. anal.;