N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide

Base Information

• Chemical Name: N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide
• CAS No.: 1232774-80-9
• Molecular Formula: C₁₅H₂₆N₃PSe
• Molecular Weight: 358.325

Synonyms:N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide

Chemical Property of N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide

Chemical Property:

Purity/Quality:

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Technology Process of N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide

There total 1 articles about N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

P-(tert-butyl)-N-phenyl-P-(trichloromethyl)phosphinoselenoic amide (1232774-61-6) + dimethyl amine (124-40-3) → N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide (1232774-80-9)

Guidance literature:

at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

Reference yield: 90.0%

N,N-dimethyl-N'-phenyl-1-(dimethylamino)-1-(tert-butyl)-phosphinecarboximidamide selenide (1232774-80-9) → 1-(dimethylamino)-1-(1,1-tert-butyl)-N,N-dimethyl-N'-phenylphosphinecarboximidamide (1232774-95-6)

Guidance literature:

With tris(morpholino)phosphine; In benzene; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

upstream raw materials:

P-(tert-butyl)-N-phenyl-P-(trichloromethyl)phosphinoselenoic amide

dimethyl amine

Downstream raw materials:

1-(dimethylamino)-1-(1,1-tert-butyl)-N,N-dimethyl-N'-phenylphosphinecarboximidamide

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