2-[hydroxy(diphenyl)methyl]phenyl N,N,N',N'-tetramethyldiamidophosphate

Base Information Edit

Chemical Name:2-[hydroxy(diphenyl)methyl]phenyl N,N,N',N'-tetramethyldiamidophosphate
CAS No.:127136-68-9
Molecular Formula:C₂₃H₂₇N₂O₃P
Molecular Weight:410.453
Hs Code.:
Mol file:127136-68-9.mol

Synonyms:C₂₃H₂₇N₂O₃P

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Chemical Property of 2-[hydroxy(diphenyl)methyl]phenyl N,N,N',N'-tetramethyldiamidophosphate Edit

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Technology Process of 2-[hydroxy(diphenyl)methyl]phenyl N,N,N',N'-tetramethyldiamidophosphate

There total 2 articles about 2-[hydroxy(diphenyl)methyl]phenyl N,N,N',N'-tetramethyldiamidophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 119-61-9
benzophenone

: 7393-13-7
(1-phenyl)-N,N,N',N'-tetramethyldiamido phosphate

: 127136-68-9
C₂₃H₂₇N₂O₃P

Guidance literature:: With sec.-butyllithium; 1.) cyclohexane, THF, -105 deg C, 1 h, 2.) cyclohexane, THF, -105 deg C, 1 h;
DOI:10.1248/cpb.38.2637

Reference yield:

: 108-95-2,27073-41-2
phenol

: 127136-68-9
C₂₃H₂₇N₂O₃P

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 1.) NaH / 1.) THF, 30 min, room temperature, 2.) THF, 12 h, room temperature

2: 72 percent / 1.) sec-BuLi / 1.) cyclohexane, THF, -105 deg C, 1 h, 2.) cyclohexane, THF, -105 deg C, 1 h

With sec.-butyllithium; sodium hydride;
DOI:10.1248/cpb.38.2637