3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

Base Information

Chemical Name:3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester
CAS No.:467217-00-1
Molecular Formula:C₃₀H₃₈O₅Si
Molecular Weight:506.714
Hs Code.:

3-(<i>tert</i>-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

Synonyms:3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

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Chemical Property of 3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

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Technology Process of 3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

There total 4 articles about 3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 467216-99-5
3-(3-dimethoxymethyl-phenyl)-3-hydroxy-propionic acid ethyl ester

: 467217-00-1
3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/S0040-4039(02)01056-0

Reference yield:

: 626-19-7
Isophthalaldehyde

: 467217-00-1
3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NH₄NO₃ / methanol / 2 h / Heating

2: 88 percent / SiO₂; aq. H₂SO₄ / CH₂Cl₂ / 0.75 h / 20 °C

3: 79 percent / LDA / tetrahydrofuran / 0.5 h / -80 °C

4: 91 percent / imidazole / dimethylformamide / 24 h / 20 °C

With 1H-imidazole; ammonium nitrate; sulfuric acid; silica gel; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01056-0

Reference yield:

: 37832-33-0
isophthalaldehyde bis-dimethylacetal

: 467217-00-1
3-(tert-butyl-diphenyl-silanyloxy)-3-(3-dimethoxymethyl-phenyl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / SiO₂; aq. H₂SO₄ / CH₂Cl₂ / 0.75 h / 20 °C

2: 79 percent / LDA / tetrahydrofuran / 0.5 h / -80 °C

3: 91 percent / imidazole / dimethylformamide / 24 h / 20 °C

With 1H-imidazole; sulfuric acid; silica gel; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01056-0