2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester
CAS No.:351377-66-7
Molecular Formula:C₁₉H₂₈O₅
Molecular Weight:336.428
Hs Code.:

Synonyms:2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Suppliers and Price of 2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

There total 6 articles about 2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-en-1-ol

: 3282-30-2
pivaloyl chloride

: 351377-66-7
2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 3h;
DOI:10.1002/anie.200503982

Reference yield:

: 886450-13-1
2-methoxymethoxy-6-methyl-phenol

: 351377-66-7
2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / K₂CO₃ / acetonitrile / 5 h / 80 °C

2: 96 percent / Me₂NPh / toluene / 12 h / 210 °C

3: 87 percent / K₂CO₃ / acetonitrile / 12 h / 80 °C

4: 99 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 25 °C

5: 99 percent / pyridine / CH₂Cl₂ / 3 h / 25 °C

With pyridine; tetrabutyl ammonium fluoride; potassium carbonate; N,N-dimethyl-aniline; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1002/anie.200503982

Reference yield:

: tert-butyl-[4-(2-methoxymethoxy-6-methyl-phenoxy)-but-2-enyloxy]-dimethyl-silane

: 351377-66-7
2,2-dimethyl-propionic acid 4-(4-methoxy-3-methoxymethoxy-5-methyl-phenyl)-but-2-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / Me₂NPh / toluene / 12 h / 210 °C

2: 87 percent / K₂CO₃ / acetonitrile / 12 h / 80 °C

3: 99 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 25 °C

4: 99 percent / pyridine / CH₂Cl₂ / 3 h / 25 °C

With pyridine; tetrabutyl ammonium fluoride; potassium carbonate; N,N-dimethyl-aniline; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1002/anie.200503982