2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

Base Information

Chemical Name:2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol
CAS No.:1593874-56-6
Molecular Formula:C₂₆H₃₈Cl₂N₂O₂
Molecular Weight:481.506
Hs Code.:

Synonyms:2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

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Chemical Property of 2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

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Technology Process of 2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

There total 5 articles about 2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 926230-89-9
2,4-dichloro-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol

: 194734-57-1
3,5-di-tert-butyl-2-hydroxybenzyl bromide

: 1593874-56-6
2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

Guidance literature:: 2,4-dichloro-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

3,5-di-tert-butyl-2-hydroxybenzyl bromide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/om500608j

Reference yield: 54.7%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 96-76-4
2,4-di-tert-Butylphenol

: 926230-89-9
2,4-dichloro-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol

: 1593874-56-6
2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

Guidance literature:: In methanol; water; for 96h; Reflux;
DOI:10.1039/c3dt53431f

Reference yield:

: 90-60-8
3,5-dichlorosalicyclaldehyde

: 1593874-56-6
2-[[[[3,5-bis-chloro-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-di-tert-butylphenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 12 h / Reflux

2.1: sodium tetrahydroborate / methanol / 2 h / 20 °C

2.2: pH 7

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran

3.2: 0 - 20 °C

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1021/om500608j