1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

Base Information

Chemical Name:1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol
CAS No.:207505-91-7
Molecular Formula:C₂₈H₃₇NO₃
Molecular Weight:435.607
Hs Code.:

Synonyms:1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

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Chemical Property of 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

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Technology Process of 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

There total 12 articles about 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

: 207505-91-7
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 25 ℃; for 1h;
DOI:10.1016/S0040-4039(98)00340-2

Reference yield:

: 197504-70-4
1-(6-amino-3,4-dimethoxy-2-methylphenyl)propan-2-yl acetate

: 207505-91-7
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) air; 2.) Me₃NO / 3.) Pd/C / 1.) MeCN, 25 deg C, 7 d; 2.) Me₂CO, 56 deg C, 4 h; 3.) o-xylene, 145 deg C, 4 h

2: NBS / CCl₄ / 0.5 h / 77 °C

3: 1.) Ni(CO)4 / 1.) C₆H₆, 65 deg C, 2.5 h; 2.) DMF, 70 deg C, 17 h

4: 98 percent / LiAlH₄ / diethyl ether / 1 h / 25 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; air; trimethylamine-N-oxide; tetracarbonyl nickel; palladium on activated charcoal; In tetrachloromethane; diethyl ether;
DOI:10.1016/S0040-4039(98)00340-2

Reference yield:

: 1845-54-1
(±)-ethyl 5-methyl-2-(prop-1-en-2-yl)hex-4-enoate

: 207505-91-7
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)(9H-carbazol-1-yl)]propan-2-ol

Guidance literature:: Multi-step reaction with 6 steps

1: NaOH / ethanol; H₂O / 20 h / 78 °C

2: 74 percent / HCOOH, H₂SO₄ / 96 h / 25 °C

3: 98 percent / LiAlH₄ / diethyl ether / 1 h / 25 °C

4: 90 percent / PBr₃, pyridine / diethyl ether / 2 h / -78 - 25 °C

5: 1.) Ni(CO)4 / 1.) C₆H₆, 65 deg C, 2.5 h; 2.) DMF, 70 deg C, 17 h

6: 98 percent / LiAlH₄ / diethyl ether / 1 h / 25 °C

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; formic acid; sulfuric acid; phosphorus tribromide; tetracarbonyl nickel; In diethyl ether; ethanol; water;
DOI:10.1016/S0040-4039(98)00340-2