1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Base Information

Chemical Name:1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate
CAS No.:207505-90-6
Molecular Formula:C₃₀H₃₉NO₄
Molecular Weight:477.644
Hs Code.:

Synonyms:1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

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Chemical Property of 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

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Technology Process of 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

There total 19 articles about 1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: π-(β-cyclolavandulyl)nickel bromide

: 197504-73-7
1-[6-bromo-3,4-dimethoxy-2-methyl-(9H-carbazol-1-yl)]propan-2-yl acetate

: 1378348-36-7
1,2-bis-(2,4,4-trimethyl-1-cyclohexen-1-yl)ethane

: 197504-72-6
1-[3,4-dimethoxy-2-methyl-(9H-carbazol-1-yl)]propan-2-yl acetate

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 17h; Inert atmosphere;
DOI:10.3998/ark.5550190.0013.323

Reference yield: 44.0%

: π-(β-cyclolavandulyl)nickel bromide

: 197504-73-7
1-[6-bromo-3,4-dimethoxy-2-methyl-(9H-carbazol-1-yl)]propan-2-yl acetate

: 1378348-36-7
1,2-bis-(2,4,4-trimethyl-1-cyclohexen-1-yl)ethane

: 937811-11-5
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylacetyl)-9H-carbazol-1-yl]propan-2-yl acetate

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.3998/ark.5550190.0013.323

Reference yield:

: 197504-70-4
1-(6-amino-3,4-dimethoxy-2-methylphenyl)propan-2-yl acetate

: 207505-90-6
1-[3,4-dimethoxy-2-methyl-6-(2,4,4-trimethyl-1-cyclohexen-1-ylmethyl)-9H-carbazol-1-yl]propan-2-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) air; 2.) Me₃NO / 3.) Pd/C / 1.) MeCN, 25 deg C, 7 d; 2.) Me₂CO, 56 deg C, 4 h; 3.) o-xylene, 145 deg C, 4 h

2: NBS / CCl₄ / 0.5 h / 77 °C

3: 1.) Ni(CO)4 / 1.) C₆H₆, 65 deg C, 2.5 h; 2.) DMF, 70 deg C, 17 h

With N-Bromosuccinimide; air; trimethylamine-N-oxide; tetracarbonyl nickel; palladium on activated charcoal; In tetrachloromethane;
DOI:10.1016/S0040-4039(98)00340-2