1H-Pyrrole-3-carboxamide,N-(2-acetylphenyl)-2,5-dimethyl-(9CI)

Base Information

Chemical Name:1H-Pyrrole-3-carboxamide,N-(2-acetylphenyl)-2,5-dimethyl-(9CI)
CAS No.:643744-39-2
Molecular Formula:C₁₅H₁₆N₂O₂
Molecular Weight:256.304
Hs Code.:
Mol file:643744-39-2.mol

Synonyms:2,5-dimethyl-1H-pyrrole-3-carboxylic acid (2-acetylphenyl)amide

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Chemical Property of 1H-Pyrrole-3-carboxamide,N-(2-acetylphenyl)-2,5-dimethyl-(9CI)

Chemical Property:

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Technology Process of 1H-Pyrrole-3-carboxamide,N-(2-acetylphenyl)-2,5-dimethyl-(9CI)

There total 3 articles about 1H-Pyrrole-3-carboxamide,N-(2-acetylphenyl)-2,5-dimethyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 551-93-9
2-aminoacetophenone

: 1000169-28-7
2,5-dimethyl-1H-pyrrole-3-carbonyl chloride

: 643744-39-2
2,5-dimethyl-1H-pyrrole-3-carboxylic acid (2-acetylphenyl)amide

Guidance literature:: In dichloromethane; at 25 ℃; for 6h;
DOI:10.1016/S0968-0896(03)00413-9

Reference yield:

: 57338-76-8
2,5-dimethyl-1H-pyrrole-3-carboxylic acid

: 643744-39-2
2,5-dimethyl-1H-pyrrole-3-carboxylic acid (2-acetylphenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 0 - 25 °C

2: 0.282 g / CH₂Cl₂ / 6 h / 25 °C

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/S0968-0896(03)00413-9

Reference yield:

: 2199-52-2
2,5-dimethyl-1H-pyrrole-3-carboxylic acid ethyl ester

: 643744-39-2
2,5-dimethyl-1H-pyrrole-3-carboxylic acid (2-acetylphenyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O

2: oxalyl chloride; DMF / CH₂Cl₂ / 0 - 25 °C

3: 0.282 g / CH₂Cl₂ / 6 h / 25 °C

With oxalyl dichloride; water; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/S0968-0896(03)00413-9