1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)
CAS No.:1257050-69-3
Molecular Formula:C₂₄H₃₀O₈S₂
Molecular Weight:510.629
Hs Code.:

Synonyms:1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

Suppliers and Price of 1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

Chemical Property:

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Technology Process of 1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

There total 10 articles about 1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1256546-72-1
[8-(hydroxymethyl)-1,4-dioxaspiro[4.5]decan-8-yl]methanol

: 98-59-9
p-toluenesulfonyl chloride

: 1257050-69-3
1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

Guidance literature:: In pyridine; at 20 ℃;
DOI:10.1021/ml500069w

Reference yield:

: C₁₀H₁₄O₆

: 98-59-9
p-toluenesulfonyl chloride

: 1257050-69-3
1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

Guidance literature:: With pyridine; at 20 ℃; Cooling with ice;

Reference yield:

: 1256546-71-0
8,8-diethyl 1,4-dioxaspiro[4.5]decane-8,8-dicarboxylate

: 1257050-69-3
1,4-dioxaspiro[4.5]decane-8,8-diylbis(methylene) bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 10 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

1.2: 1.5 h / -5 - 30 °C

2.1: pyridine / dmap / 48 h / 20 °C

With pyridine; lithium aluminium tetrahydride; dmap; In tetrahydrofuran;