C₁₄H₁₃N₅O

Base Information

Chemical Name:C₁₄H₁₃N₅O
CAS No.:1400807-98-8
Molecular Formula:C₁₄H₁₃N₅O
Molecular Weight:267.29
Hs Code.:

C<sub>14</sub>H<sub>13</sub>N<sub>5</sub>O

Synonyms:C₁₄H₁₃N₅O

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Chemical Property of C₁₄H₁₃N₅O

Chemical Property:

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Technology Process of C₁₄H₁₃N₅O

There total 6 articles about C₁₄H₁₃N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1400807-97-7
C₁₃H₁₁N₅O

: 74-88-4
methyl iodide

: 1400807-98-8
C₁₄H₁₃N₅O

Guidance literature:: C₁₃H₁₁N₅O; With potassium carbonate; In acetone; at 20 ℃; for 0.333333h;

methyl iodide; In acetone; at 45 ℃; for 1h;

Reference yield:

: 27828-71-3
5-hydroxynicotinic acid

: 1400807-98-8
C₁₄H₁₃N₅O

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / Reflux

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C

3.1: ethanol / 70 °C / Sealed tube

4.1: thionyl chloride / N,N-dimethyl-formamide / 1 h / 0 °C

5.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 14 h / 100 °C

6.1: potassium carbonate / acetone / 0.33 h / 20 °C

6.2: 1 h / 45 °C

With thionyl chloride; sodium azide; potassium carbonate; ammonium chloride; triphenylphosphine; diethylazodicarboxylate; sulfuric acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 30766-22-4
methyl 5-hydroxy-3-pyridinecarboxylate

: 1400807-98-8
C₁₄H₁₃N₅O

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C

2.1: ethanol / 70 °C / Sealed tube

3.1: thionyl chloride / N,N-dimethyl-formamide / 1 h / 0 °C

4.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 14 h / 100 °C

5.1: potassium carbonate / acetone / 0.33 h / 20 °C

5.2: 1 h / 45 °C

With thionyl chloride; sodium azide; potassium carbonate; ammonium chloride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetone;