C₃₃H₃₆BrN₃O₈

Base Information

Chemical Name:C₃₃H₃₆BrN₃O₈
CAS No.:115288-87-4
Molecular Formula:C₃₃H₃₆BrN₃O₈
Molecular Weight:682.568
Hs Code.:

C<sub>33</sub>H<sub>36</sub>BrN<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₃H₃₆BrN₃O₈

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Chemical Property of C₃₃H₃₆BrN₃O₈

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Technology Process of C₃₃H₃₆BrN₃O₈

There total 20 articles about C₃₃H₃₆BrN₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 115288-87-4
C₃₃H₃₆BrN₃O₈

Guidance literature:: Multi-step reaction with 18 steps

1: i-Pr₂NEt / 1,2-dichloro-ethane / 70 °C

2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / -78 °C

3: NH₃ / methanol / Ambient temperature

4: 82 percent / Et₃N, DMAP / CH₂Cl₂ / 24 h / -20 °C

5: NaBH₄ / methanol; CH₂Cl₂ / -20 °C

6: HgCl₂, CSA / acetonitrile; H₂O / 0.33 h / 40 °C

7: 59 percent / NaBH₄ / methanol; CH₂Cl₂ / 0 °C

8: H₂ / Ra-Ni (W₂) / ethanol / 1.5 h / 100 °C / 103430 Torr

9: NaHCO₃ / ethanol / Ambient temperature

10: 78 percent / Br₂ / CH₂Cl₂ / Ambient temperature

11: 100 percent / pyridine / 0.17 h / 60 °C

12: 92 percent / DMAP, Et₃N / 1,2-dichloro-ethane / 0.5 h / 80 °C

13: 97 percent / NaBH₄ / methanol / 0 °C

14: 97 percent / n-Bu₄NF / tetrahydrofuran / Ambient temperature

15: Ambient temperature

16: methanol / 0.33 h / 120 °C

17: 83 percent / K₂CO₃ / acetone / 2 h / Ambient temperature

18: 1) (COCl)2, Et₃N; 2) ZnCl₂ / 1) DMSO, CH₂Cl₂, -78 deg C; 2) CH₂Cl₂, r. t.

With pyridine; dmap; sodium tetrahydroborate; oxalyl dichloride; camphor-10-sulfonic acid; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; hydrogen; bromine; sodium hydrogencarbonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; zinc(II) chloride; Ra-Ni (W₂); In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja00223a052

Reference yield:

: 115288-69-2
3-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-benzaldehyde

: 115288-87-4
C₃₃H₃₆BrN₃O₈

Guidance literature:: Multi-step reaction with 17 steps

1: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / -78 °C

2: NH₃ / methanol / Ambient temperature

3: 82 percent / Et₃N, DMAP / CH₂Cl₂ / 24 h / -20 °C

4: NaBH₄ / methanol; CH₂Cl₂ / -20 °C

5: HgCl₂, CSA / acetonitrile; H₂O / 0.33 h / 40 °C

6: 59 percent / NaBH₄ / methanol; CH₂Cl₂ / 0 °C

7: H₂ / Ra-Ni (W₂) / ethanol / 1.5 h / 100 °C / 103430 Torr

8: NaHCO₃ / ethanol / Ambient temperature

9: 78 percent / Br₂ / CH₂Cl₂ / Ambient temperature

10: 100 percent / pyridine / 0.17 h / 60 °C

11: 92 percent / DMAP, Et₃N / 1,2-dichloro-ethane / 0.5 h / 80 °C

12: 97 percent / NaBH₄ / methanol / 0 °C

13: 97 percent / n-Bu₄NF / tetrahydrofuran / Ambient temperature

14: Ambient temperature

15: methanol / 0.33 h / 120 °C

16: 83 percent / K₂CO₃ / acetone / 2 h / Ambient temperature

17: 1) (COCl)2, Et₃N; 2) ZnCl₂ / 1) DMSO, CH₂Cl₂, -78 deg C; 2) CH₂Cl₂, r. t.

With pyridine; dmap; sodium tetrahydroborate; oxalyl dichloride; camphor-10-sulfonic acid; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; hydrogen; bromine; sodium hydrogencarbonate; potassium carbonate; triethylamine; mercury dichloride; zinc(II) chloride; Ra-Ni (W₂); In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja00223a052

Reference yield:

: 1,4-Diacetyl-3-prop-2-ynyl-piperazine-2,5-dione

: 115288-87-4
C₃₃H₃₆BrN₃O₈

Guidance literature:: Multi-step reaction with 18 steps

1: AIBN / benzene

2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / -78 °C

3: NH₃ / methanol / Ambient temperature

4: 82 percent / Et₃N, DMAP / CH₂Cl₂ / 24 h / -20 °C

5: NaBH₄ / methanol; CH₂Cl₂ / -20 °C

6: HgCl₂, CSA / acetonitrile; H₂O / 0.33 h / 40 °C

7: 59 percent / NaBH₄ / methanol; CH₂Cl₂ / 0 °C

8: H₂ / Ra-Ni (W₂) / ethanol / 1.5 h / 100 °C / 103430 Torr

9: NaHCO₃ / ethanol / Ambient temperature

10: 78 percent / Br₂ / CH₂Cl₂ / Ambient temperature

11: 100 percent / pyridine / 0.17 h / 60 °C

12: 92 percent / DMAP, Et₃N / 1,2-dichloro-ethane / 0.5 h / 80 °C

13: 97 percent / NaBH₄ / methanol / 0 °C

14: 97 percent / n-Bu₄NF / tetrahydrofuran / Ambient temperature

15: Ambient temperature

16: methanol / 0.33 h / 120 °C

17: 83 percent / K₂CO₃ / acetone / 2 h / Ambient temperature

18: 1) (COCl)2, Et₃N; 2) ZnCl₂ / 1) DMSO, CH₂Cl₂, -78 deg C; 2) CH₂Cl₂, r. t.

With pyridine; dmap; sodium tetrahydroborate; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); camphor-10-sulfonic acid; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; hydrogen; bromine; sodium hydrogencarbonate; potassium carbonate; triethylamine; mercury dichloride; zinc(II) chloride; Ra-Ni (W₂); In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; acetone; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1021/ja00223a052