Technology Process of C30H26N2O5
There total 6 articles about C30H26N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diphenyl phosphoryl azide; triethylamine;
In
toluene;
at 80 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere
2.1: water; sodium hydroxide / tetrahydrofuran / 20 °C
2.2: pH 4.0
3.1: chloro-trimethyl-silane / 48 h / 0 - 20 °C
4.1: diphenyl phosphoryl azide; triethylamine / toluene / 80 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; water; sodium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tert.-butylnitrite; boron trifluoride diethyl etherate / tetrahydrofuran / -30 - -5 °C
1.2: 0.25 h / 20 °C
2.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / Inert atmosphere; Reflux
4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere
5.1: water; sodium hydroxide / tetrahydrofuran / 20 °C
5.2: pH 4.0
6.1: chloro-trimethyl-silane / 48 h / 0 - 20 °C
7.1: diphenyl phosphoryl azide; triethylamine / toluene / 80 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; chloro-trimethyl-silane; tert.-butylnitrite; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; water; potassium acetate; sodium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; toluene;