{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

Base Information

Chemical Name:{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate
CAS No.:1301763-98-3
Molecular Formula:C₃₈H₆₂N₄O₁₁
Molecular Weight:750.93
Hs Code.:

{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

Synonyms:{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

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Chemical Property of {(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

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Technology Process of {(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

There total 3 articles about {(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 124-38-9,18923-20-1
carbon dioxide

: 1301763-78-9
chloromethyl (4S,5S)-5-((2S)-2-{[(3-amino-2,2-dimethyl-3-oxopropyl)amino]carbonyl}-3-methylbutyl)-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidine-3-carboxylate

: 1301763-98-3
{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

Guidance literature:: morpholine; carbon dioxide; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

chloromethyl (4S,5S)-5-((2S)-2-{[(3-amino-2,2-dimethyl-3-oxopropyl)amino]carbonyl}-3-methylbutyl)-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidine-3-carboxylate; In N,N-dimethyl-formamide; for 30h;

Reference yield:

: 173334-57-1
(2S,4S,5S,7S)-5-Amino-4-hydroxy-2-isopropyl-7-[4-methoxy-3-(3-methoxy-propoxy)-benzyl]-8-methyl-nonanoic acid (2-carbamoyl-2-methyl-propyl)-amide

: 1301763-98-3
{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; tetrahydrofuran / Cooling with ice

1.2: 0.5 h / Cooling with ice

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2.2: 30 h

With caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: (2S,4S,5S,7S)-N-(2-carbamoyl-2-methylpropyl)-5-amino-4-hydroxy-2,7-diisopropyl-8-[4-methoxy-3-(3-methoxypropoxy)phenyl]octanamide hemifumarate

: 1301763-98-3
{(4S,5S)-5-[(2S)-2-(3-amino-2,2-dimethyl-3-oxopropylaminocarbonyl)-3-methylbutyl]-4-{(2S)-2-[4-methoxy-3-(3-methoxypropoxy)benzyl]-3-methylbutyl}-1,3-oxazolidin-3-yl-carbonyloxy}methyl morpholine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / water / 20 °C

1.2: 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2.2: 30 h

With sodium carbonate; caesium carbonate; In water; N,N-dimethyl-formamide;