N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide
CAS No.:85763-09-3
Molecular Formula:C₁₃H₁₄F₃N₃O₄
Molecular Weight:333.267
Hs Code.:

Synonyms:N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

Suppliers and Price of N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

Chemical Property:

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Technology Process of N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

There total 4 articles about N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 302-17-0
chloral hydrate

: 81654-49-1
N-[2-(3-amino-4-methoxyphenyl)ethyl]-2,2,2-trifluoro acetamide

: 85763-09-3
N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

Guidance literature:: With hydroxyammonium sulfate; sulfuric acid; In water; for 0.0666667h; Heating;
DOI:10.1021/jm00361a001

Reference yield:

: 81654-47-9
2,2,2-Trifluoro-N-[2-(4-methoxyphenyl)ethyl]acetamide

: 85763-09-3
N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 84.5 percent / HNO₃, TFA / 2 h / Ambient temperature

2: 76.3 percent / hydrazine hydrate / Raney nickel / ethanol / 2 h / 15 °C

3: 68 percent / aq. H₂SO₄, hydroxylamine sulfate / 0.07 h / Heating

With sulfuric acid; nitric acid; hydroxylamine sulfate; hydrazine hydrate; trifluoroacetic acid; nickel; In ethanol;
DOI:10.1021/jm00156a010

Reference yield:

: 81654-48-0
N-<2-(4-methoxy-3-nitrophenyl)ethyl>-2,2,2-trifluoroacetamide

: 85763-09-3
N-<2-<3-<(hydroximinoacetyl)amino>-4-methoxyphenyl>ethyl>-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76.3 percent / hydrazine hydrate / Raney nickel / ethanol / 2 h / 15 °C

2: 68 percent / aq. H₂SO₄, hydroxylamine sulfate / 0.07 h / Heating

With sulfuric acid; hydroxylamine sulfate; hydrazine hydrate; nickel; In ethanol;
DOI:10.1021/jm00156a010