C₁₂H₁₉N₂O₄P

Base Information

• Chemical Name: C₁₂H₁₉N₂O₄P
• CAS No.: 133642-10-1
• Molecular Formula: C₁₂H₁₉N₂O₄P
• Molecular Weight: 286.268
• Mol file: 133642-10-1.mol

Synonyms:C₁₂H₁₉N₂O₄P

Chemical Property of C₁₂H₁₉N₂O₄P

Chemical Property:

Purity/Quality:

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Technology Process of C₁₂H₁₉N₂O₄P

There total 1 articles about C₁₂H₁₉N₂O₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + o-Tolyl N,N,N',N'-tetramethylphosphorodiamidate (56184-99-7) → C12H19N2O4P (133642-10-1)

Guidance literature:

With sec.-butyllithium; Yield given. Multistep reaction; 1.) THF, -105 deg C, 1 h, 2.) -105 deg C;

DOI:10.1248/cpb.39.41

Reference yield: 54.0%

C12H19N2O4P (133642-10-1) → benzofuran-2(3H)-one (553-86-6)

Guidance literature:

With formic acid; for 1h; Heating;

DOI:10.1248/cpb.39.41

upstream raw materials:

carbon dioxide

o-Tolyl N,N,N',N'-tetramethylphosphorodiamidate

Downstream raw materials:

benzofuran-2(3H)-one

Refernces