1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

Base Information

Chemical Name:1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide
CAS No.:266338-88-9
Molecular Formula:C₃₅H₅₁N₅O₆
Molecular Weight:637.82
Hs Code.:

1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

Synonyms:1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

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Chemical Property of 1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

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Technology Process of 1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

There total 8 articles about 1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-84-5
1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

: 266338-88-9
1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: In acetonitrile; at 20 ℃; for 92h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 529-64-6,28845-94-5
Tropic acid

: 266338-88-9
1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

4: 100 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

5: 92 percent / acetonitrile / 72 h / 20 °C

6: 95 percent / aq. HCl / tetrahydrofuran / 4.5 h / 40 °C

7: 95 percent / acetonitrile / 92 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition / 4: Hydrolysis / 5: Addition / 6: Hydrolysis / 7: Addition;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-88-9
1-[1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxamido]-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

4: 100 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

5: 92 percent / acetonitrile / 72 h / 20 °C

6: 95 percent / aq. HCl / tetrahydrofuran / 4.5 h / 40 °C

7: 95 percent / acetonitrile / 92 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition / 4: Hydrolysis / 5: Addition / 6: Hydrolysis / 7: Addition;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1