1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

Base Information

Chemical Name:1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid
CAS No.:266338-84-5
Molecular Formula:C₂₇H₃₇N₃O₆
Molecular Weight:499.607
Hs Code.:

Synonyms:1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

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Chemical Property of 1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

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Technology Process of 1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

There total 7 articles about 1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 266338-80-1
1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)-N,N-dimethylcyclopentanecarboxamide

: 266338-84-5
1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 40 ℃; for 4.5h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 529-64-6,28845-94-5
Tropic acid

: 266338-84-5
1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

4: 100 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

5: 92 percent / acetonitrile / 72 h / 20 °C

6: 95 percent / aq. HCl / tetrahydrofuran / 4.5 h / 40 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition / 4: Hydrolysis / 5: Addition / 6: Hydrolysis;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-84-5
1-(1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxamido)cyclopentanecarboxilic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

4: 100 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

5: 92 percent / acetonitrile / 72 h / 20 °C

6: 95 percent / aq. HCl / tetrahydrofuran / 4.5 h / 40 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition / 4: Hydrolysis / 5: Addition / 6: Hydrolysis;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1