5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

Base Information

Chemical Name:5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide
CAS No.:1173693-35-0
Molecular Formula:C₁₂H₁₂F₂N₂O₂
Molecular Weight:254.236
Hs Code.:

Synonyms:5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

Suppliers and Price of 5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

There total 1 articles about 5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30558-50-0
2-(dimethylamino)-N-hydroxy-2-oxoethanimidoylchloride

: 207226-37-7,791521-82-9
1,3-difluoro-2-vinyl-benzene

: 1173693-35-0
5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

Guidance literature:: With potassium carbonate; In water; chlorobenzene; at 10 - 15 ℃;

Reference yield:

: 1173693-35-0
5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

: 75-16-1
methylmagnesium bromide

: 1173693-36-1
1-[5-(2,6-difluorophenyl)-4,5-dihydro-1,2-oxazol-3-yl]ethan-1-one

Guidance literature:: 5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide; methylmagnesium bromide; In tetrahydrofuran; toluene; at -10 - -5 ℃;

With hydrogenchloride; water; In tetrahydrofuran; toluene; at 10 - 35 ℃;

Reference yield:

: 1173693-35-0
5-(2,6-difluorophenyl)-4,5-dihydro-N,N-dimethyl-3-isoxazolecarboxamide

: 1313705-27-9
1,2-diethyl 4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2-thiazolyl]tetrahydro-1,2-pyridazinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; toluene / -10 - -5 °C

2: bromine / dichloromethane / 5 - 33 °C

3: methanol / 1 h / 45 - 50 °C

With bromine; In tetrahydrofuran; methanol; dichloromethane; toluene;