6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Base Information

Chemical Name:6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol
CAS No.:113347-78-7
Molecular Formula:C₁₉H₁₇N₃O
Molecular Weight:303.363
Hs Code.:

Synonyms:6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Suppliers and Price of 6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

There total 4 articles about 6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 113377-62-1
(Z)-α-(1,2,3,4-Tetrahydro-β-carbolin-2-yl)-acetophenonoxim

: 113347-78-7
6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Guidance literature:: With edetate disodium; mercury(II) oxide; In ethanol; at 80 - 90 ℃; for 1h;
DOI:10.1007/BF00809930

Reference yield:

: 16502-01-5
tetrahydrobetacarboline

: 113347-78-7
6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / tetrahydrofuran / 1 h

2: 3 g / NH₂OH*HCl / ethanol / 3 h / Heating

3: 55 percent / HgO/Na₂EDTA*2H₂O / ethanol / 1 h / 80 - 90 °C

With hydroxylamine hydrochloride; edetate disodium; mercury(II) oxide; In tetrahydrofuran; ethanol;
DOI:10.1007/BF00809930

Reference yield:

: 111733-93-8
α-(1,2,3,4-Tetrahydro-β-carbolin-2-yl)-acetophenon

: 113347-78-7
6,7,12,12b-Tetrahydro-3-phenyl-4H-<1,2,5>-oxadiazino<5',6':1,2>pyrido<3,4-b>indol

Guidance literature:: Multi-step reaction with 2 steps

1: 3 g / NH₂OH*HCl / ethanol / 3 h / Heating

2: 55 percent / HgO/Na₂EDTA*2H₂O / ethanol / 1 h / 80 - 90 °C

With hydroxylamine hydrochloride; edetate disodium; mercury(II) oxide; In ethanol;
DOI:10.1007/BF00809930