tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

Base Information

Chemical Name:tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside
CAS No.:364781-14-6
Molecular Formula:C₅₇H₆₀O₁₀
Molecular Weight:905.097
Hs Code.:

Synonyms:tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

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Chemical Property of tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

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Technology Process of tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

There total 3 articles about tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 106-95-6
allyl bromide

: 364781-15-7
1',2,3,3',4',6'-hexa-O-benzyl-6-deoxy-6-iodo-sucrose

: 364781-14-6
tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM

Reference yield:

: 89499-92-3
2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

: 364781-14-6
tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / aq. AcOH / acetone / 0.5 h / 80 °C

2: 93 percent / I₂; Ph₃P; imidazole / toluene / 2.5 h / 70 °C

3: 88 percent / NaH / dimethylformamide / 18 h / 20 °C

With 1H-imidazole; iodine; sodium hydride; acetic acid; triphenylphosphine; In N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM

Reference yield:

: 89499-93-4
2,3-di-O-benzyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

: 364781-14-6
tetra-O-benzyl-2'-O-(4-O-allyl-2,3-di-O-benzyl-6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / I₂; Ph₃P; imidazole / toluene / 2.5 h / 70 °C

2: 88 percent / NaH / dimethylformamide / 18 h / 20 °C

With 1H-imidazole; iodine; sodium hydride; triphenylphosphine; In N,N-dimethyl-formamide; toluene;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM