2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Chemical Name:2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside
CAS No.:89499-92-3
Molecular Formula:C₅₇H₆₂O₁₁
Molecular Weight:923.113
Hs Code.:

Synonyms:2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Chemical Property of 2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Technology Process of 2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

There total 3 articles about 2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 60825-19-6
4,6-O-isopropylidene sucrose hexabenzoate

: 100-44-7
benzyl chloride

: 89499-92-3
2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/0008-6215(84)85160-5

Reference yield: 56.0%

: 100-39-0
benzyl bromide

: 71196-27-5
4,6-mono-O-isopropylidene sucrose

: 89499-92-3
2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM

Reference yield:

: 98-88-4
benzoyl chloride

: 89499-92-3
2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 93 percent / NaH / dimethylformamide / Ambient temperature

With pyridine; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85160-5