Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

Base Information

Chemical Name:Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester
CAS No.:204857-56-7
Molecular Formula:C₂₃H₃₈ClNO₅S
Molecular Weight:476.077
Hs Code.:

Synonyms:Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

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Chemical Property of Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

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Technology Process of Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

There total 3 articles about Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 112-31-2
caprinaldehyde

: 204857-35-2
N-(tert-butoxycarbonyl)-N-(4-chlorobenzyl)-methanesulfonamide

: 204857-56-7
Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; 1.) -78 deg C, 1 h, 2.) -78 to 20 deg C, 1 h;
DOI:10.1055/s-1998-1609

Reference yield:

: 42060-30-0
N-(4-chloro-benzyl)-methanesulfonamide

: 204857-56-7
Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / CH₂Cl₂

2: 74 percent / t-BuOK / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) -78 to 20 deg C, 1 h

With dmap; potassium tert-butylate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1998-1609

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 204857-56-7
Carbonic acid tert-butyl ester 1-[(4-chloro-benzylsulfamoyl)-methyl]-decyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂

2: DMAP / CH₂Cl₂

3: 74 percent / t-BuOK / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) -78 to 20 deg C, 1 h

With dmap; potassium tert-butylate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1998-1609