2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

Base Information

Chemical Name:2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester
CAS No.:1176272-70-0
Molecular Formula:C₂₁H₂₈N₂O₃S
Molecular Weight:388.531
Hs Code.:

Synonyms:2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

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Chemical Property of 2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

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Technology Process of 2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

There total 1 articles about 2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1176272-67-5
8-(2,4,6-trimethylphenyl)hexahydropyrazolo[1,2-d][1,4,5]thiadiazepine-7,9-dione

: 3282-30-2
pivaloyl chloride

: 1176272-70-0
2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2008.12.062

Reference yield: 100.0%

: 1176272-70-0
2,2-dimethylpropionic acid 9-oxo-8-(2,4,6-trimethylphenyl)-1,2,4,5-tetrahydro-9H-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

: 1176272-72-2
2,2-dimethylpropionic acid 3,9-dioxo-8-(2,4,6-trimethylphenyl)-2,3,4,5-tetrahydro-1H,9H-3λ4-pyrazolo[1,2-d][1,4,5]thiadiazepin-7-yl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 5 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmc.2008.12.062